To ensure the accuracy of data when testing the elastic modulus of silicone resin, the following key aspects can be addressed:
Sample preparation process
Dimensional accuracy control: Prepare specimens strictly in accordance with relevant standards (such as ASTM, GB/T, etc.). Whether it is dumbbell shaped specimens for tensile testing, cylindrical or cubic specimens for compression testing, or rectangular specimens for bending testing, their length, width, thickness, diameter, and other dimensional parameters must be accurately controlled. Use high-precision measuring tools (such as vernier calipers, micrometers, etc.) for measurement to ensure that dimensional errors are within the allowable range of the standard, as deviations in sample size can directly affect subsequent stress and strain calculations, thereby affecting the accuracy of elastic modulus.
Sample quality assurance: Ensure that the surface of the sample is smooth and flat, without obvious defects such as bubbles, cracks, impurities, etc. During the sample preparation process, such as using injection molding, compression molding, and other methods, it is necessary to control the process parameters well to ensure that the silicone resin is evenly filled into the mold, avoiding stress concentration caused by internal defects, which may lead to deviations in the test results. For samples with special requirements, corresponding post-processing (such as grinding, polishing, etc.) is also required to make them meet the testing requirements.
Experimental environment control
Temperature regulation: Maintain a constant temperature in the testing environment, as temperature has a significant impact on the mechanical properties of silicone resin. In an ideal situation, the temperature should be controlled at the standard specified temperature (such as 23 ℃± 2 ℃), and high-precision constant temperature and humidity chambers can be used to create a stable temperature environment, avoiding temperature fluctuations that may cause changes in the elastic modulus of silicone resin, thereby ensuring that the test data can truly reflect its performance at specific temperatures.
Humidity management: It is also necessary to control the environmental humidity. High humidity may cause silicone resin to absorb moisture, which in turn affects its physical, chemical, and mechanical properties, resulting in inaccurate elastic modulus test results. It is advisable to maintain a relative humidity of 40% -60% in general indoor environments, and adjust the humidity through devices such as dehumidifiers and humidifiers to ensure that the humidity remains stable within the appropriate range.
Calibration and maintenance of experimental equipment
Calibration instruments: Regularly calibrate the testing equipment used (such as tensile testing machines, compression testing machines, bending testing machines, dynamic mechanics analyzers, etc.) to ensure accurate measurement of key components such as force sensors and displacement sensors. Calibration work should be carried out by qualified professional metrology institutions in accordance with relevant metrology regulations, obtaining calibration certificates to ensure the accuracy and reliability of force values, displacement and other data measured by equipment, and providing accurate raw data for subsequent elastic modulus calculations.
Equipment maintenance: Carry out daily maintenance of the equipment, keep the testing machine fixtures clean and flexible, and prevent problems such as fixture wear and jamming from affecting the clamping and force uniformity of the samples; For precision instruments such as dynamic mechanics analyzers, it is necessary to regularly clean the internal optical path, inspect the circuit system, etc., to ensure that the instrument is in good operating condition and avoid erroneous data caused by equipment failures.
Test operation specifications
Sample clamping: When installing the sample, it is necessary to strictly follow the operating instructions of the equipment to ensure that the sample is firmly clamped and evenly stressed on the testing machine. For example, in tensile testing, the axis of the specimen should be completely aligned with the direction of tension to avoid eccentric tension, otherwise it will cause excessive local stress in the specimen, abnormal stress-strain curves, and affect the accuracy of elastic modulus calculation.
Reasonable parameter settings: Based on the characteristics of silicone resin and relevant standards, correctly set the loading speed, frequency (for dynamic mechanical analysis, etc.), temperature range (if involving variable temperature testing) and other parameters for the experiment. If the loading speed is too fast, it may not be possible to accurately record the data of the elastic deformation stage. If the speed is too slow, it will affect the efficiency of the test and may introduce other interference factors. Therefore, it is necessary to choose a reasonable speed to ensure that the test process can accurately reflect the true elastic properties of the silicone resin.
Repeated test: For the same batch of silicone resin materials, multiple repeated tests (generally not less than 3 times) are conducted, and the average value is taken as the final elastic modulus result. Through multiple experiments, data fluctuations caused by individual differences in samples, accidental errors in experimental operations, and other factors can be reduced, improving the reliability and accuracy of the results.
Rigorous data processing
Accurately recording raw data: During the experiment, it is necessary to carefully and completely record the raw data output by the testing machine, such as force values, displacement, time, temperature, etc., to avoid omissions and errors, and ensure accurate basis for subsequent data processing.
Correct calculation and analysis: According to the corresponding mechanical calculation formulas and theories, accurately calculate parameters such as stress, strain, and elastic modulus. In the process of drawing stress-strain curves and other analysis, appropriate fitting methods and software tools should be selected to ensure the accuracy of the curve and accurately determine the value of elastic modulus. At the same time, it is necessary to analyze and judge the rationality of the data. If abnormal data occurs, the cause should be identified (such as experimental operation errors, defects in the sample, etc.), and if necessary, the test should be repeated.
What are the specific steps for sharing and testing the elastic modulus of silicone resin? Are the elastic modulus results of silicone resin obtained by different testing methods the same? How to choose suitable testing equipment to measure the elastic modulus of silicone resin?
Room termperature curing polysilazane, pls check
IOTA 9150, IOTA 9150K.
High termperature curing polysilazane, pls check
IOTA 9108,
IOTA 9118.